Identified XRD reflections in TSRC-1 and TSRC-2 blends
| 2θ: degrees | Identified phase (see Table 4 for ICDD numbers) | |||||
|---|---|---|---|---|---|---|
| Control | Acid treated, core | Acid treated, surface | ||||
| TSRC-1 | TSRC-2 | TSRC-1 | TSRC-2 | TSRC-1 | TSRC-2 | |
| — | — | 12·05 | 12·07 | — | — | Dminsteinbergite |
| — | — | 12·47 | — | 12·47 | — | Garronite |
| 14·58 | 14·44 | 14·56 | 14·46 | 14·55 | 14·59 | Boehmite |
| — | — | — | 14·75 | — | 14·75 | Bassanite |
| — | — | — | — | 15·41 | 15·54 | Alunite |
| — | — | — | 15·86 | — | — | Analcime |
| — | — | 16·48 | 16·3 | 16·35 | 16·35 | Mullite |
| 17·62 | 17·46 | — | 17·56 | — | — | Katoite |
| — | — | 18·02 | — | 17·88 | 17·98 | Garronite/alunite |
| — | — | — | 18·34 | — | — | Analcime |
| — | — | 20·10 | 20·08/20·11 | — | 20·08 | Dminsteinbergite/gypsum |
| 20·14 | 20·18 | 20·18 | 20·1 | 20·1 | 20·16 | Quartz |
| 20·38 | 20·20 | — | 20·20 | — | — | Katoite |
| — | — | 21·5 | — | 21·5 | — | Garronite |
| — | — | 22·02 | — | 22·02 | — | Garronite |
| — | — | 23·48 | 23·38 | 23·4 | 23·50 | Dminsteinbergite |
| — | — | 24·18 | 24·12 | 24·0 | 24·1/24·16 | Dminsteinbergite/hematite |
| — | — | — | 25·50 | — | 25·42 | Anhydrate |
| 25·74 | — | 25·74 | — | 25·56 | 25·48 | Corundum/alunite |
| — | — | — | 25·86 | — | 25·76–26·0 | Bassanite |
| — | — | 26·08 | 26·05 | — | — | Analcime |
| 26·32 | 26·22 | 26·32 | 26·2 | 26·19/26·32 | 25·9–26·3 | Quartz/mullite |
| — | — | 26·62 | — | 26·62 | 26·6 | Quartz |
| 26·98 | 26·86 | 26·98 | 26·99 | — | — | Katoite |
| — | — | 27·8 | — | — | — | Garronite |
| 28·16 | 28·18 | 28·12 | 28·1 | 28·18 | 28·18 | Quartz |
| 28·29 | 28·23 | 28·29 | 28·14 | 28·29 | 28·22 | Garronite/boehmite |
| 28·86 | 28·76 | — | 28·9/28·84 | — | — | Katoite/gypsum/quartz |
| 29·5 | 29·4 | 29·5 | 29·34 | — | — | Calcium carbonate |
| — | — | — | 29·48 | — | 29·8–30·2 | Bassanite |
| — | — | — | — | 29·90 | 30·1 | Alunite |
| — | — | — | 30·64/30·3 | — | 30·36 | Analcime/hematite |
| — | — | — | 31·34 | — | 31·36 | Anhydrate |
| — | — | — | — | 31·36 | 31·37 | Alunite |
| — | 31·40 | — | 31·40 | — | 31·4 | Gehlenite |
| — | — | 31·63 | 31·58 | — | 31·62 | Dminsteinbergite |
| — | — | — | 31·7 | — | 31·8 | Bassanite |
| 32·38 | 32·24 | — | 32·39 | — | — | Katoite |
| 33·28 | 33·12 | 33·26 | 33·14 | 33·08/33·28 | 33·12/33·3 | Perovskite/iron oxide/mullite |
| — | — | 33·60 | — | 33·60 | — | Garronite |
| — | — | 35·16 | 35·14 | — | 35·20 | Dminsteinbergite |
| 35·22 | 35·4 | 35·22 | 35·2 | 35·22 | 36·2 | Corundum/mullite |
| 36·1 | 36·1 | 35·78 | 35·9/35·68 | — | 35·9–35·8 | Dminsteinbergite/hematite |
| 37·06 | 36·88 | — | 37·08 | — | — | Katoite |
| 37·9 | — | 37·7 | — | 37·7 | — | Corundum |
| 38·42 | 38·3 | 38·42 | 38·33 | 38·42 | 38·36 | Boehmite |
| 39·5 | 39·36 | 39·4 | 39·4 | 39·73 | 39·4–39·8/39·6 | Alunite/calcium carbonate |
| — | — | — | 39·58 | — | 39·7 | Bassanite |
| — | — | 39·82 | 39·88 | 40·0 | 39·72 | Dminsteinbergite |
| 39·85 | 39·72 | — | 39·95 | — | — | Katoite |
| 41·0 | 41·15 | 40·8/40·87 | 40·8/40·9 | 40·75 | 40·75/40·8 | Iron oxide/calcium carbonate/mullite/anhydrate |
| — | — | 42·10 | 42·00 | — | 42·1 | Dminsteinbergite |
| — | — | 42·71 | 42·63 | — | 42·75 | Dminsteinbergite |
| — | — | — | 42·95 | — | 42·3–42·8 | Bassanite |
| 43·47 | — | 43·31 | — | 43·31 | — | Corundum |
| 45·11 | 45·01 | — | 45·22 | — | — | Katoite |
| — | 47·59 | — | 47·51/47·24–47·55 | — | 47·3–47·4 | Perovskite/calcium carbonate |
| — | — | — | — | 47·65 | 47·80 | Alunite |
| 48·99 | 48·87 | — | 48·89 | — | 48·9–49·2 | Boehmite |
| 49·47 | 49·21 | 49·27–49·40 | 49·33 | 49·27 | 49·2–49·3 | Dminsteinbergite/quartz/boehmite |
| 2 | Identified phase | |||||
|---|---|---|---|---|---|---|
| Control | Acid treated, core | Acid treated, surface | ||||
| TSRC-1 | TSRC-2 | TSRC-1 | TSRC-2 | TSRC-1 | TSRC-2 | |
| — | — | 12·05 | 12·07 | — | — | Dminsteinbergite |
| — | — | 12·47 | — | 12·47 | — | Garronite |
| 14·58 | 14·44 | 14·56 | 14·46 | 14·55 | 14·59 | Boehmite |
| — | — | — | 14·75 | — | 14·75 | Bassanite |
| — | — | — | — | 15·41 | 15·54 | Alunite |
| — | — | — | 15·86 | — | — | Analcime |
| — | — | 16·48 | 16·3 | 16·35 | 16·35 | Mullite |
| 17·62 | 17·46 | — | 17·56 | — | — | Katoite |
| — | — | 18·02 | — | 17·88 | 17·98 | Garronite/alunite |
| — | — | — | 18·34 | — | — | Analcime |
| — | — | 20·10 | 20·08/20·11 | — | 20·08 | Dminsteinbergite/gypsum |
| 20·14 | 20·18 | 20·18 | 20·1 | 20·1 | 20·16 | Quartz |
| 20·38 | 20·20 | — | 20·20 | — | — | Katoite |
| — | — | 21·5 | — | 21·5 | — | Garronite |
| — | — | 22·02 | — | 22·02 | — | Garronite |
| — | — | 23·48 | 23·38 | 23·4 | 23·50 | Dminsteinbergite |
| — | — | 24·18 | 24·12 | 24·0 | 24·1/24·16 | Dminsteinbergite/hematite |
| — | — | — | 25·50 | — | 25·42 | Anhydrate |
| 25·74 | — | 25·74 | — | 25·56 | 25·48 | Corundum/alunite |
| — | — | — | 25·86 | — | 25·76–26·0 | Bassanite |
| — | — | 26·08 | 26·05 | — | — | Analcime |
| 26·32 | 26·22 | 26·32 | 26·2 | 26·19/26·32 | 25·9–26·3 | Quartz/mullite |
| — | — | 26·62 | — | 26·62 | 26·6 | Quartz |
| 26·98 | 26·86 | 26·98 | 26·99 | — | — | Katoite |
| — | — | 27·8 | — | — | — | Garronite |
| 28·16 | 28·18 | 28·12 | 28·1 | 28·18 | 28·18 | Quartz |
| 28·29 | 28·23 | 28·29 | 28·14 | 28·29 | 28·22 | Garronite/boehmite |
| 28·86 | 28·76 | — | 28·9/28·84 | — | — | Katoite/gypsum/quartz |
| 29·5 | 29·4 | 29·5 | 29·34 | — | — | Calcium carbonate |
| — | — | — | 29·48 | — | 29·8–30·2 | Bassanite |
| — | — | — | — | 29·90 | 30·1 | Alunite |
| — | — | — | 30·64/30·3 | — | 30·36 | Analcime/hematite |
| — | — | — | 31·34 | — | 31·36 | Anhydrate |
| — | — | — | — | 31·36 | 31·37 | Alunite |
| — | 31·40 | — | 31·40 | — | 31·4 | Gehlenite |
| — | — | 31·63 | 31·58 | — | 31·62 | Dminsteinbergite |
| — | — | — | 31·7 | — | 31·8 | Bassanite |
| 32·38 | 32·24 | — | 32·39 | — | — | Katoite |
| 33·28 | 33·12 | 33·26 | 33·14 | 33·08/33·28 | 33·12/33·3 | Perovskite/iron oxide/mullite |
| — | — | 33·60 | — | 33·60 | — | Garronite |
| — | — | 35·16 | 35·14 | — | 35·20 | Dminsteinbergite |
| 35·22 | 35·4 | 35·22 | 35·2 | 35·22 | 36·2 | Corundum/mullite |
| 36·1 | 36·1 | 35·78 | 35·9/35·68 | — | 35·9–35·8 | Dminsteinbergite/hematite |
| 37·06 | 36·88 | — | 37·08 | — | — | Katoite |
| 37·9 | — | 37·7 | — | 37·7 | — | Corundum |
| 38·42 | 38·3 | 38·42 | 38·33 | 38·42 | 38·36 | Boehmite |
| 39·5 | 39·36 | 39·4 | 39·4 | 39·73 | 39·4–39·8/39·6 | Alunite/calcium carbonate |
| — | — | — | 39·58 | — | 39·7 | Bassanite |
| — | — | 39·82 | 39·88 | 40·0 | 39·72 | Dminsteinbergite |
| 39·85 | 39·72 | — | 39·95 | — | — | Katoite |
| 41·0 | 41·15 | 40·8/40·87 | 40·8/40·9 | 40·75 | 40·75/40·8 | Iron oxide/calcium carbonate/mullite/anhydrate |
| — | — | 42·10 | 42·00 | — | 42·1 | Dminsteinbergite |
| — | — | 42·71 | 42·63 | — | 42·75 | Dminsteinbergite |
| — | — | — | 42·95 | — | 42·3–42·8 | Bassanite |
| 43·47 | — | 43·31 | — | 43·31 | — | Corundum |
| 45·11 | 45·01 | — | 45·22 | — | — | Katoite |
| — | 47·59 | — | 47·51/47·24–47·55 | — | 47·3–47·4 | Perovskite/calcium carbonate |
| — | — | — | — | 47·65 | 47·80 | Alunite |
| 48·99 | 48·87 | — | 48·89 | — | 48·9–49·2 | Boehmite |
| 49·47 | 49·21 | 49·27–49·40 | 49·33 | 49·27 | 49·2–49·3 | Dminsteinbergite/quartz/boehmite |
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