Specimen conditions and test results of XRD tests
| Group no. | wi: % | 2θ_3w: degrees | d001_3w: nm | 2θ_os: degrees | d001_os: nm |
|---|---|---|---|---|---|
| XRD_wi | 29·4 | 4·66 | 1·90 | — | — |
| 32·4 | 4·62 | 1·91 | — | — | |
| 34·6 | 4·64 | 1·90 | — | — | |
| 35·5 | 4·64 | 1·90 | — | — | |
| 41·5 | 4·64 | 1·90 | 2·30 | 3·84 | |
| 46·0 | 4·6 | 1·92 | 2·25 | 3·93 | |
| 46·3 | 4·62 | 1·91 | 2·36 | 3·74 | |
| 51·7 | 4·62 | 1·91 | 2·26 | 3·91 | |
| 52·9 | 4·62 | 1·91 | 2·20 | 4·02 | |
| 57·2 | 4·6 | 1·92 | 2·16 | 4·09 | |
| 57·6 | 4·58 | 1·93 | 2·18 | 4·05 | |
| 64·3 | 4·42 | 2·00 | 2·14 | 4·13 | |
| 64·8 | 4·3 | 2·05 | 2·06 | 4·29 | |
| 72·4 | — | — | 2·02 | 4·37 | |
| 76·6 | — | — | 1·86 | 4·75 | |
| 76·7 | — | — | 1·94 | 4·55 | |
| 95·7 | — | — | 1·67 | 5·29 | |
| 95·9 | — | — | 1·70 | 5·20 | |
| 102·8 | — | — | 1·60 | 5·52 | |
| 102·9 | — | — | 1·60 | 5·52 |
| Group no. | 2 | 2 | |||
|---|---|---|---|---|---|
| XRD_ | 29·4 | 4·66 | 1·90 | — | — |
| 32·4 | 4·62 | 1·91 | — | — | |
| 34·6 | 4·64 | 1·90 | — | — | |
| 35·5 | 4·64 | 1·90 | — | — | |
| 41·5 | 4·64 | 1·90 | 2·30 | 3·84 | |
| 46·0 | 4·6 | 1·92 | 2·25 | 3·93 | |
| 46·3 | 4·62 | 1·91 | 2·36 | 3·74 | |
| 51·7 | 4·62 | 1·91 | 2·26 | 3·91 | |
| 52·9 | 4·62 | 1·91 | 2·20 | 4·02 | |
| 57·2 | 4·6 | 1·92 | 2·16 | 4·09 | |
| 57·6 | 4·58 | 1·93 | 2·18 | 4·05 | |
| 64·3 | 4·42 | 2·00 | 2·14 | 4·13 | |
| 64·8 | 4·3 | 2·05 | 2·06 | 4·29 | |
| 72·4 | — | — | 2·02 | 4·37 | |
| 76·6 | — | — | 1·86 | 4·75 | |
| 76·7 | — | — | 1·94 | 4·55 | |
| 95·7 | — | — | 1·67 | 5·29 | |
| 95·9 | — | — | 1·70 | 5·20 | |
| 102·8 | — | — | 1·60 | 5·52 | |
| 102·9 | — | — | 1·60 | 5·52 |
Note: 2θ_3w and d001_3w are diffraction peak angle and basal spacing corresponding to hydration state of 3w; 2θ_os and d001_os are diffraction peak angle and basal spacing corresponding to osmotic swelling.
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