A new process for the manufacture of a novel hydraulic binder (Celitement) with a high potential for saving energy and reducing carbon dioxide emissions was developed at the Karlsruhe Institute of Technology. To obtain the ideal process conditions and to monitor the optimal product quality of the binder, it was necessary to develop a measurement system for the online determination of certain quality parameters. A method for the direct calculation of different quality parameters of both precursor and final product from online measured near-infrared (NIR) spectra is presented in this article. A successful transformation between calibration models gained with laboratory and online NIR is also demonstrated. This enables optimisation of the calibration models on a laboratory scale and a seamless transfer to industrial scale due to changes in composition of the raw materials, formulation or processing parameters.
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Research Article|
February 15 2018
Celitement quality parameter determination by online NIR spectroscopy Available to Purchase
Carolin Lutz;
Carolin Lutz
Institute for Applied Computer Science, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Jörg Matthes;
Jörg Matthes
Institute for Applied Computer Science, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany (corresponding author: joerg.matthes@kit.edu)
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Patrick Waibel;
Patrick Waibel
Institute for Applied Computer Science, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Ulrich Precht;
Ulrich Precht
Institute for Technical Chemistry, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Günther Beuchle;
Günther Beuchle
Institute for Technical Chemistry, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Krassimir Garbev;
Krassimir Garbev
Institute for Technical Chemistry, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Uwe Schweike;
Uwe Schweike
Institute for Technical Chemistry, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Peter Stemmermann;
Peter Stemmermann
Institute for Technical Chemistry, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Hubert B. Keller
Hubert B. Keller
Institute for Applied Computer Science, Karlsruhe Institute of Technology, Eggenstein-Leopoldshafen, Germany
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Publisher: Emerald Publishing
Received:
January 23 2017
Revision Received:
December 14 2017
Accepted:
December 15 2017
Online ISSN: 1751-7605
Print ISSN: 0951-7197
ICE Publishing: All rights reserved
2018
Advances in Cement Research (2019) 31 (2): 80–91.
Article history
Received:
January 23 2017
Revision Received:
December 14 2017
Accepted:
December 15 2017
Citation
Lutz C, Matthes J, Waibel P, Precht U, Beuchle G, Garbev K, Schweike U, Stemmermann P, Keller HB (2019), "Celitement quality parameter determination by online NIR spectroscopy". Advances in Cement Research, Vol. 31 No. 2 pp. 80–91, doi: https://doi.org/10.1680/jadcr.17.00016
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