Chemical vapor deposition processes to create magnesium diboride (MgB2) nanowires, a well-known superconductor, and orthorhombic boron nanorods are reported. These boron nanorods are doped with magnesium and sulfur, and the doping induces a number of defects in the material. The synthesis technique used to create these materials is based on a method used originally to create a variety of pure boron nanomaterials. The addition of sulfur and ammonia dramatically alters the process, resulting in new products. The morphology of these materials was characterized with scanning and transmission electron microscopy. Electron energy loss spectroscopy, electron diffraction and Fourier transform analysis were performed to determine crystal spacings and chemical composition of both materials. MgB2 nanowires especially, because of their superconducting nature and small dimensions, have a number of interesting uses. This article contains supporting information that available online.
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October 2014
Research Article|
October 01 2014
Synthesis of MgB2 nanowires and doped orthorhombic boron nanorods Available to Purchase
Rajen B. Patel;
Rajen B. Patel
*
Materials Science and Engineering, New Jersey Institute of Technology, Newark, NJ, USA
*Corresponding author e-mail address: rajenbp@gmail.com
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Tsengming Chou;
Tsengming Chou
Laboratory for Multiscale Imaging, Stevens Institute of Technology, Hoboken, NJ, USA
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Zafar Iqbal
Zafar Iqbal
Materials Science and Engineering, New Jersey Institute of Technology, Newark, NJ, USA
Department of Chemistry and Environmental Science, New Jersey Institute of Technology, Newark, NJ, USA
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*Corresponding author e-mail address: rajenbp@gmail.com
Publisher: Emerald Publishing
Received:
January 22 2014
Accepted:
May 21 2014
Online ISSN: 2046-0155
Print ISSN: 2046-0147
ICE Publishing: All rights reserved
2014
Emerging Materials Research (2014) 3 (5): 217–221.
Article history
Received:
January 22 2014
Accepted:
May 21 2014
Citation
Patel RB, Chou T, Iqbal Z (2014), "Synthesis of MgB2 nanowires and doped orthorhombic boron nanorods". Emerging Materials Research, Vol. 3 No. 5 pp. 217–221, doi: https://doi.org/10.1680/emr.14.00003
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