Foamed bitumen stabilisation (FBS) is widely used to enhance durability, moisture resistance, and road flexibility while reducing cracking. Addressing knowledge gaps in its application with recycled materials can expand their usage in road construction. This study focused on stabilising mixes of 50% recycled concrete aggregate (RCA) and 50% fine recycled glass (RG) using foamed bitumen (FB). Recycled toner aggregate (RTA) and geopolymers derived from ground granulated blast furnace slag (S) and fly ash (FA) were evaluated as potential alternatives to conventional secondary binders, such as Portland cement for FBS of recycled material blends. To assess the performance of RTA, a fixed 3% FB dosage was combined with varying RTA amounts (1%–4%). Geopolymers including FA, S, and (FA + S) at dosages of 10%, 20%, and 30% by mass of RCA and RG blend were tested alongside 3% FB for their stabilising effectiveness. FB-stabilised samples with RTA initially failed the indirect tensile modulus tests, but their performance improved significantly after extended curing. The blend incorporating geopolymers, RCA + RG + 3% FB + 20% (FA + S), met local road authority standards. These results demonstrate the potential of sustainable secondary binders for the stabilisation of RCA and RG mixtures in road construction.
Introduction
With the growing emphasis on building environmentally sustainable roads, the construction industry is increasingly focusing on the reuse of construction and demolition (C&D) waste. Governments worldwide are promoting sustainability by encouraging the reduction, reuse, and recycling of all types of waste to decrease the consumption of natural resources. In 2022–2023, Australia generated approximately 26.8 million tonnes of C&D waste and 1.36 million tonnes of glass waste. The resource recovery rate for C&D waste reached 84%, yet 16% still ended up in landfills without reuse. Similarly, while the recycling rate for glass waste remained constant at 61%, 39% of this material was landfilled (Pickin et al., 2024). Recycled concrete aggregate (RCA) is a primary product derived from C&D waste. While some glass containers can be recycled back into new glass products, others cannot, which complicates waste disposal efforts. Fine recycled glass (RG) has found wide application in road construction, where it serves as a sustainable alternative to natural sand. Numerous studies have been conducted to evaluate the suitability of various recycled materials for road construction, aiming to prevent C&D waste from going to landfill (Arulrajah et al., 2014, Alnedawiet al., 2021; Maghool et al., 2021).
A widely accepted practice in Australasia is the stabilisation of granular pavement materials and underlying soils. This process involves the mechanical incorporation of reactive agents to enhance the materials’ properties (Browne, 2020). Traditional pavement stabilisation often uses high cement content, resulting in a stiff, fully bound base layer prone to shrinkage cracks. Although slower-setting additives are now used to reduce stiffness, the focus on achieving high unconfined compressive strength (UCS) values still leads to cracking issues (Ramanujam et al., 2007). A variety of research studies have explored the performance of stabilised recycled materials using a range of chemical stabilisation methods (Senanayake et al., 2022; Mohammadinia et al., 2017; Maghool et al., 2022). According to a research, the key stabilisation additives that help prevent fatigue cracking are lime–fly ash (FA), emulsion with cement, and foamed bitumen (FB) (Ramanujam and Jones, 2007).
Bitumen stabilisation is achieved by mixing bitumen, either as foam or emulsion, with granular materials, either in a plant or through in situ stabilisation. The purpose of bituminous stabilisation is to add cohesion to non-plastic materials or to reduce the moisture sensitivity of cohesive materials to enhance their stability and mechanical properties (Austroads, 2019). FB is created by injecting a small amount of cold, finely misted water into hot penetration grade bitumen within an expansion chamber. This process temporarily lowers the viscosity of the bitumen, allowing it to mix effectively with aggregates at ambient temperature and existing moisture levels (Jenkins et al., 2000). Foamed bitumen stabilisation (FBS) is considered more flexible than other stabilisation treatments, with the aim of creating a road pavement that is strong, flexible, and impermeable. A study indicated that FBS is a cost-effective alternative to traditional cement, lime stabilisation methods (Saleh, 2007). Research conducted using the Accelerated Pavement Testing Facility demonstrated that natural granular material stabilised with 1.2%–2.8% FB and 1% cement exhibited better performance, with reduced rutting, compared to stabilisation using only cement (1%) or only FB (2.2%) (Gonzalez et al., 2009).
In earlier study, the performance of these FB-stabilised blends of RCA, which were mixed with RG, recycled plastic, and reclaimed asphalt pavement (RAP) was assessed through experimental testing. The results showed that indirect tensile strength, UCS, and California bearing ratio (CBR) values decreased with increasing RAP, RG, and recycled plastic contents. Compared to unbound blends, the FB-stabilised mixtures showed improved resistance to permanent deformation, attributed to the combined effects of FB and the filler, hydrated lime (Maghool et al., 2022). In a separate investigation, FA and asphalt emulsion were utilised to create a stabilised mixture of marginal crushed rock, with the objective of enhancing the mechanical performance of low-grade materials for use as a sustainable pavement base. Compared to cement-stabilised crushed rock with a comparable UCS, the FA asphalt emulsion stabilised mixture demonstrated superior flexural strength, indirect tensile strength, resilient modulus, and fatigue life under indirect tensile loading, while also exhibiting a reduced carbon footprint (Yaowarat et al., 2021).
A study examined the flexural fatigue behaviour of FB-stabilised crushed rock mixtures under varying conditions, including temperature, bitumen content, secondary binders, density, and moisture levels, with the goal of creating a more robust design method for FB-stabilised pavements. The findings revealed that the flexural fatigue life of FB-stabilised beams improved as density and bitumen content increased but declined with rising temperature and moisture content (Pitawala et al., 2022). Research revealed that FB-stabilised materials exhibited significant behavioural changes with even a one-degree variation from the initial test temperature. It is essential to account for temperature variations in both mix and pavement designs involving these materials. The same study demonstrated that the FB-stabilised mixture exhibited a significant increase in resistance to failure and elastic modulus after an extended curing period (Dal Ben et al., 2014). A study comparing field constructed and laboratory manufactured FB-stabilised beams revealed that field samples were less sensitive to temperature and frequency changes than their laboratory counterparts (Pitawala et al., 2021.). A study demonstrated that the FB-stabilised mixture, composed of 50% crushed rock and 50% RAP, exhibited strong rut resistance, even with the high proportion of recycled content. Laboratory wheel tracking tests conducted on the field material at an elevated temperature of 60°C also confirmed its excellent rut resistance (Bodin et al., 2020).
Research evidence supports the use of waste toner, and geopolymers as a secondary binder in asphalt mixtures; but evidence of its application as a secondary binder for stabilising base or subbase pavement materials is limited. A study found that a mixture of residual toner powder and 10% calcite served as a good bitumen additive, enhancing the material’s application properties (Vucinic et al., 2013). Studies have shown that incorporating waste toner into asphalt binder enhances its stiffness, decreases moisture susceptibility, and reduces its potential for pumping. The inclusion of waste toner reduced the workability and moisture-induced damage resistance of asphalt mixtures, while improving their resistance to rutting (Huang et al., 2021). In one example, adding waste toner to pavement aggregate led to workability issues, including challenges with rolling and flaking caused by insufficient adhesion (Solaimanian et al., 1998).
Geopolymers offer a sustainable alternative to traditional cementitious systems, providing comparable mechanical properties while reducing environmental impact compared to Portland cement (Duxson et al., 2007). Numerous studies have been conducted on FA and ground granulated blast furnace slag (S)-based geopolymer stabilisation of pavements containing RCA, crushed brick, RAP, and other recycled materials. These studies demonstrated that S-based geopolymer stabilisation achieved higher compressive strength compared to FA-based geopolymer stabilisation (Doan et al., 2024; Mohammadinia et al., 2016). However, limited research has focused on the use of FA and S geopolymers as secondary binders in FBS. In a study, S-based geopolymer was used as a secondary binder for in situ FBS of 100% RAP. The results showed that incorporating S-based geopolymer led to a significant improvement in tensile strength and also caused a notable reduction in moisture resistance (Barisoglu et al., 2023). In a separate study, 0%–5% FA was intended for use as a filler in the FBS of a crushed rock and crushed limestone mix. However, preliminary investigations revealed that FA did not enhance the mechanical strength of the mix and functioned only as a mineral filler to support gradation (Jitsangiam et al., 2011). Existing literature explaining current trends in FBS, including geopolymer stabilisation, is summarised in Table 1.
Summary of literature on current trends in FBS of recycled materials on pavements
| Author | Research objectives | Recycled materials utilised | Key findings and associated advantages | Key findings and associated challenges |
|---|---|---|---|---|
| Maghool et al., 2022 | Evaluate strength and deformation of FB-stabilised waste materials | RCA, RAP, RG, and recycled plastic | FB and hydrated lime mixtures showed improved deformation resistance due to synergistic effects | Higher RAP, RG, and recycled plastic contents reduced strength |
| Bodin et al., 2020 | Study deformation of FBS materials and effects of RAP increase | 50% RAP with crushed rock | Minimal pavement surface deformation and low rates of deformation under accelerated loading in both early-life and cured states | Adding 50% RAP raised deformation rate but stayed below the control asphalt at similar temperatures |
| Doan et al., 2024 | Evaluate one-part FA and S geopolymers for stabilising C&D aggregates | RCA, crushed brick and RAP | Strength gains occurred at 0.1 activator ratio for CB and RCA, and 0.05 for RAP, exceeding traditional geopolymersLonger curing improved one-part geopolymer strength more than higher temperatures | Low fine contents notably reduced strength, especially at 10% precursor dosage |
| Mohammadinia et al., 2016 | Investigate geopolymer-stabilised C&D materials using FA and S with varied activator-to-binder ratios | RCA, crushed brick and RAP | Geopolymer stabilisation was most effective for RCA, with S binders giving higher strength than FA binders | Crushed brick had low strength, with 7-day curing and additives showing little improvement |
| Barisoglu et al., 2023 | Evaluate cold-recycled FB mixes with 100% RAP for base layers | 100% RAP | S-based geopolymer boosted tensile strength, and all active fillers improved moisture resistance by 30%–35% | Adding S-based geopolymers with FB didn’t raise wet indirect tensile strength but reduced moisture sensitivity |
| Author | Research objectives | Recycled materials utilised | Key findings and associated advantages | Key findings and associated challenges |
|---|---|---|---|---|
| Evaluate strength and deformation of FB-stabilised waste materials | RCA, RAP, RG, and recycled plastic | Higher RAP, RG, and recycled plastic contents reduced strength | ||
| Study deformation of | 50% | Minimal pavement surface deformation and low rates of deformation under accelerated loading in both early-life and cured states | Adding 50% | |
| Evaluate one-part | RCA, crushed brick and | Strength gains occurred at 0.1 activator ratio for | Low fine contents notably reduced strength, especially at 10% precursor dosage | |
| Investigate geopolymer-stabilised C&D materials using | RCA, crushed brick and | Geopolymer stabilisation was most effective for RCA, with S binders giving higher strength than | Crushed brick had low strength, with 7-day curing and additives showing little improvement | |
| Evaluate cold-recycled | 100% | S-based geopolymer boosted tensile strength, and all active fillers improved moisture resistance by 30%–35% | Adding S-based geopolymers with |
This study investigated the stabilisation of mixes containing RCA and RG using 3% FB, supplemented with alternative secondary binders such as 1%, 2%, 3%, and 4% recycled toner aggregate (RTA) and 10%, 20%, and 30% geopolymers S, FA and (FA + S) by mass of RCA and RG blend. The strength and stiffness properties of the stabilised blends were assessed in the laboratory through a series of UCS, CBR, and indirect tensile modulus (ITMr) tests.
Materials and methods
This study evaluated the potential of stabilising blends of 50% RCA and 50% fine RG using FB. The FBS process involved adding supplementary cementitious secondary binders, such RTA, which derived from waste toner and post-consumer recycled soft plastics and geopolymers made from industrial waste products such as S and FA.
As an initial step in this research, the geotechnical properties of unbound RCA and RG mixes were obtained. Figure 1 shows the unbound RCA and RG mixture and the blending apparatus. A modified Proctor compaction test was performed on unbound RCA and RG mixtures to obtain the relationship between moisture content and dry density of the blends (SA, 2017). Particle size distribution (PSD) test was performed for both unwashed and washed unbound blends (SA, 2009). For PSDs, the requirements of the local road authority (LRA), VicRoads, were adhered to, as correct distribution is important for improving compaction, enhancing load-bearing capacity, increasing durability, and optimising permeability. The Los Angeles (LA) abrasion test was conducted on the coarser fraction of the unbound blend to assess the hardness of the source material (ASTM, 2006). The flakiness index test was conducted on the unbound blend to measure the proportion of elongated or flaky particles, which aids in improving pavement compaction and stability (SA, 1999).
The image displays two separate views of different aggregate materials. The first image shows a flat, rectangular container filled with small stones and gravel, arranged evenly across the bottom. The second image depicts the interior of a processing machine, where larger stones are mixed with finer particles in a compartmentalised structure. The machine has clamping mechanisms on the sides, and the surface appears dusty, indicating previous use. Both images illustrate different states of aggregate materials, highlighting variations in size and containment.(a) Unbound RCA and RG mixture. (b) Blending apparatus
The image displays two separate views of different aggregate materials. The first image shows a flat, rectangular container filled with small stones and gravel, arranged evenly across the bottom. The second image depicts the interior of a processing machine, where larger stones are mixed with finer particles in a compartmentalised structure. The machine has clamping mechanisms on the sides, and the surface appears dusty, indicating previous use. Both images illustrate different states of aggregate materials, highlighting variations in size and containment.(a) Unbound RCA and RG mixture. (b) Blending apparatus
It is important to ensure that the foaming characteristics of FB are sufficient to adequately coat the fine particles with bitumen. In this study, the characteristics of Class 170 bitumen, the expansion ratio and half-life, were determined based on parameters established in previous research (Maghool et al., 2022). The expansion ratio quantifies the ratio of the maximum volume attained by FB to its initial volume prior to foaming. The half-life, on the other hand, refers to the time required for the FB volume to decrease to half of its maximum value (Austroads, 2017a). An increase in water content raises the expansion ratio value while reducing the half-life value. Conversely, lower water content results in highly viscous FB, leading to a lower expansion ratio value. Higher water content decreases viscosity, thereby increasing the expansion ratio value. A longer half-life allows the mixture additional time before settling occurs. Guided by prior research (Maghool et al., 2022) and supported by economic and environmental considerations, the optimal FB parameters listed in Table 2 were selected for stabilising mixtures containing 50% RCA and 50% RG.
Optimum FB parameters for C170 bitumen (Maghool et al., 2022)
| Parameters | Set value |
|---|---|
| Optimum foaming moisture content: % | 3.0 |
| Optimum foamed bitumen content: % | 3.0 |
| Foaming agent: % | 0.5 |
| Air pressure: bars | 5 |
| Water pressure: bars | 6 |
| Bitumen temperature: °C | 175–180 |
| Parameters | Set value |
|---|---|
| Optimum foaming moisture content: % | 3.0 |
| Optimum foamed bitumen content: % | 3.0 |
| Foaming agent: % | 0.5 |
| Air pressure: bars | 5 |
| Water pressure: bars | 6 |
| Bitumen temperature: °C | 175–180 |
In the second phase of the research, tests were conducted to determine the strength and resilient modulus characteristics of stabilised blends consisting of 50% RCA and 50% RG, with FB and varying contents of RTA as secondary binders. The Austroads test method, AGPT/T302, was followed for mixing materials for FBS (Austroads, 2017b). The FB was created using the Wirtgen WLB 10S machine, which is depicted in Figure 2. The formation of FB mixes involved injecting hot bitumen, together with a specified amount of cold water and compressed air, into a mixer containing the RCA and RG blend. An optimal FB content of 3.0% was chosen and applied throughout all testing phases. The application of 3% FB in pavement stabilisation is widely adopted, supported by substantial prior research (Halles et al., 2009). This proportion typically provides adequate coverage of the fines and sand particles within the pavement material, ensuring an optimal balance between the layer’s stiffness and flexibility. RTA was incorporated as an active secondary binder in quantities of 1%, 2%, 3%, and 4% by mass of RCA and RG blend to promote uniform dispersion of FB within the mixture. A 0.5% foaming agent was added to enhance the properties of the FB. In this phase, a blend containing a traditional secondary binder, cement (C), in the composition RCA + RG + 3% FB + 2% C, was used as the control. The optimum moisture content (OMC) and maximum dry density (MDD) were obtained for all five blends, including the control, using the modified Proctor compaction test (SA, 2017). The CBR tests were conducted under soaked conditions to evaluate the strength of the above mentioned five mixtures (SA, 2014). UCS tests were conducted on stabilised samples cured at 20°C and 40°C, each for a duration of 3 days (SA, 2008). The ITMr tests were conducted on the same blends to determine the ITMr values at three conditions: initially after 3 h of drying at room temperature, after 3 days of drying with curing at 40°C, and after 3 days of drying with curing at 40°C, followed by 10 min of soaking prior to testing (SA, 1995). During ITMr testing, a cyclic vertical compressive load was added in alignment with the vertical diametral plane, and horizontal displacements were recorded at the midpoint of the horizontal diameter (Austroads, 2019). The specimens were compacted using a standard Marshall mould, applying 50 blows per side. Testing began with five initial load pulses to measure the seating force, followed by an additional five cycles to evaluate the resilient modulus, using peak force and horizontal deformation data. Figure 3 illustrates the ITMr test sample along with the testing setup. The resilient modulus was obtained from Equation 1 (Austroads, 2017c):
The image displays a Wirtgen W L B 10 S machine, prominently featuring a control panel with multiple buttons in various colours, three pressure gauges, and an emergency stop button. The machine has a sloped top with safety warning labels, and there is a black bucket positioned nearby, likely used for collecting debris or materials. The overall setup indicates a workshop environment with visible floor and wall features, enhancing the context of industrial use.Laboratory-scale apparatus used to create FB
The image displays a Wirtgen W L B 10 S machine, prominently featuring a control panel with multiple buttons in various colours, three pressure gauges, and an emergency stop button. The machine has a sloped top with safety warning labels, and there is a black bucket positioned nearby, likely used for collecting debris or materials. The overall setup indicates a workshop environment with visible floor and wall features, enhancing the context of industrial use.Laboratory-scale apparatus used to create FB
The image depicts a laboratory compression testing machine designed for testing cylindrical concrete samples. The apparatus features a top plate that exerts pressure onto the concrete specimen positioned centrally on a lower frame, supported by a set of metal arms. The sample appears cylindrical and is situated between two horizontal plates, with visible compression areas. The machine includes a pressurised piston and various mechanical components for stabilisation. A black cable extends from the machine, indicating connectivity to instrumentation. The background is a uniform green, enhancing focus on the equipment and the concrete specimen being tested.ITMr testing setup and sample
The image depicts a laboratory compression testing machine designed for testing cylindrical concrete samples. The apparatus features a top plate that exerts pressure onto the concrete specimen positioned centrally on a lower frame, supported by a set of metal arms. The sample appears cylindrical and is situated between two horizontal plates, with visible compression areas. The machine includes a pressurised piston and various mechanical components for stabilisation. A black cable extends from the machine, indicating connectivity to instrumentation. The background is a uniform green, enhancing focus on the equipment and the concrete specimen being tested.ITMr testing setup and sample
where P represents the peak load, v is Poisson’s ratio (assumed to be 0.4), H denotes the recovered horizontal deformation, and hc is the average height of the specimen.
In the third stage of the research, tests were conducted to determine the strength and stiffness characteristics of stabilised mixtures composed of RCA and RG, with 3% FB and varying contents (10%, 20%, and 30%) of geopolymers as sustainable secondary binders. Figure 4 presents the physical appearance of FB material along with the secondary binder materials FA and S used in this study. Commercially available class F FA, S, and a 50:50 blend of FA and S were utilised as solid precursors (P) in the alkali activation process for geopolymer production. A liquid alkaline activator (L), consisting of a combination of sodium hydroxide (NaOH) and sodium silicate (Na2SiO3) solutions, was utilised to facilitate the alkali activation of FA, S, and the (FA + S) blend. For effective strength development and practical application, the optimal concentration of NaOH solution is reported to range between 8 and 12 mol. In this study, a concentration of 8 mol was selected, considering both economic and safety considerations (Hanjitsuwan et al., 2014, Rattanasak et al., 2009, Arulrajah et al., 2018). The Na2SiO3 solution used in this study was a commercially available D-grade liquid Na2SiO3 with a molar ratio of 2. Based on previous studies, the optimal ratios for strength development in alkali-activated FA and S were found to be 70:30 for Na2SiO3:NaOH and 0.4 for L/P, and the same ratios were adopted for this study (Lin et al., 2023). In this stage, nine mixtures – RCA + RG + 3% FB + 10%, 20%, and 30% FA; RCA + RG + 3% FB + 10%, 20%, and 30% S; and RCA + RG + 3% FB + 10%, 20%, and 30% (FA + S) – were evaluated using modified compaction, CBR, UCS, and ITMr tests. Figure 5 presents the sequential testing procedure adopted in this study, illustrating the various material compositions and the laboratory tests conducted under different conditions across different stages.
The image comprises three sequential pictures labelled a, b, and c. The first image, a, shows a black, viscous substance inside a dark bowl, with visible surface textures reflecting light. The second image, b, features a grey, granular powder within a circular container, displaying a smooth, even surface. The third image, c, showcases a white, fine powder in a similar container to b, exhibiting a soft, undisturbed surface. Each container appears to have a circular shape, with consistent dimensions across the images, and the backgrounds are neutral and metallic, possibly indicating a laboratory or workshop environment.(a) Foamed bitumen. (b) Fly ash, and (c) slag used in testing
The image comprises three sequential pictures labelled a, b, and c. The first image, a, shows a black, viscous substance inside a dark bowl, with visible surface textures reflecting light. The second image, b, features a grey, granular powder within a circular container, displaying a smooth, even surface. The third image, c, showcases a white, fine powder in a similar container to b, exhibiting a soft, undisturbed surface. Each container appears to have a circular shape, with consistent dimensions across the images, and the backgrounds are neutral and metallic, possibly indicating a laboratory or workshop environment.(a) Foamed bitumen. (b) Fly ash, and (c) slag used in testing
The image presents a flowchart detailing a three stage experimental process aimed at assessing the geotechnical properties and stabilisation techniques for a mix involving unbound Recycled Concrete Aggregate and Recycled Glass in equal proportions. Stage one outlines the assessment of the geotechnical properties of the unbound mix and the determination of foaming characteristics of Class 170 bitumen, referencing parameters from a previous study. Stage two describes the evaluation of stabilised parent mixes using three per cent of Fly Ash Brick and Reclaimed Asphalt, at one to four per cent, including specified tests for California Bearing Ratio, Unconfined Compressive Strength at two temperatures, and Indirect Tensile Strength. It details drying and curing protocols following the tests. Stage three focuses on evaluating stabilised mixes with three per cent Fly Ash Brick and Geopolymers, indicating types and proportions of Geopolymers, alongside similar testing and curing processes. The flowchart features directional arrows indicating the process flow and includes boxed text for clarity.Stages of laboratory testing
The image presents a flowchart detailing a three stage experimental process aimed at assessing the geotechnical properties and stabilisation techniques for a mix involving unbound Recycled Concrete Aggregate and Recycled Glass in equal proportions. Stage one outlines the assessment of the geotechnical properties of the unbound mix and the determination of foaming characteristics of Class 170 bitumen, referencing parameters from a previous study. Stage two describes the evaluation of stabilised parent mixes using three per cent of Fly Ash Brick and Reclaimed Asphalt, at one to four per cent, including specified tests for California Bearing Ratio, Unconfined Compressive Strength at two temperatures, and Indirect Tensile Strength. It details drying and curing protocols following the tests. Stage three focuses on evaluating stabilised mixes with three per cent Fly Ash Brick and Geopolymers, indicating types and proportions of Geopolymers, alongside similar testing and curing processes. The flowchart features directional arrows indicating the process flow and includes boxed text for clarity.Stages of laboratory testing
Results and discussion
The 50% RCA and 50% RG unbound blend was considered the parent material for the series of stabilisation tests conducted for this research. The OMC and MDD of the unbound mixture were 9.22% and 2.081 t/m³, respectively, and the compaction curve is presented in Figure 6. The LA abrasion value for the recycled material source was 26, the flakiness index of the material was 13, and both values met the LRA’s requirements for base and subbase materials (Vicroads, 2018; Vicroads, 2017a). PSD analyses were performed for both washed and unwashed unbound blends. The results, along with the LRA recommended grading envelope for upper and lower subbase materials, are presented in Figure 7. The grading of the unwashed blend, which was most relevant to the research, fell within the allowable grading envelope (Vicroads, 2017a). Accordingly, the unbound blend of 50% RCA and 50% RG met the necessary LRA requirements for FBS.
The graph illustrates the relationship between dry density, measured in tonnes per cubic metre, and moisture content, percentages. The X axis represents moisture content, ranging from seven point five to eleven point five percent, while the Y axis represents dry density, ranging from two point zero five to two point zero nine tonnes per cubic metre. A smooth curve connects several plotted data points, illustrating the trend between the two variables. In the top left corner, annotations indicate the maximum dry density, M D D, as two point zero eight one tonnes per cubic metre and the optimum moisture content, O M C, as nine point two two percent. The curve starts at a lower density at low moisture levels, increases to a peak, and then gradually declines, indicating the relationship between these variables.Dry density plotted against moisture content for the unbound RCA + RG blend
The graph illustrates the relationship between dry density, measured in tonnes per cubic metre, and moisture content, percentages. The X axis represents moisture content, ranging from seven point five to eleven point five percent, while the Y axis represents dry density, ranging from two point zero five to two point zero nine tonnes per cubic metre. A smooth curve connects several plotted data points, illustrating the trend between the two variables. In the top left corner, annotations indicate the maximum dry density, M D D, as two point zero eight one tonnes per cubic metre and the optimum moisture content, O M C, as nine point two two percent. The curve starts at a lower density at low moisture levels, increases to a peak, and then gradually declines, indicating the relationship between these variables.Dry density plotted against moisture content for the unbound RCA + RG blend
The graph illustrates the particle size distribution of a blend, comparing washed and unwashed materials. The X axis represents sieve sizes measured in millimetres, ranging from zero point zero one to ten. The Y axis shows the percentage of passing particles, ranging from zero to one hundred percent. Three distinct lines are plotted, a solid black line for unwashed samples, a solid green line for washed samples, and dotted blue and red lines indicating upper and lower specification limits, respectively, cited from Vicroads, 2017 a. Data points for each line are represented by shapes, triangles for unwashed, squares for washed, and x marks for specification limits. The graph exhibits a consistent increase in percentage passing as the sieve size increases, with the unwashed samples consistently higher than the washed.Particle size distribution of unbound RCA and RG blend
The graph illustrates the particle size distribution of a blend, comparing washed and unwashed materials. The X axis represents sieve sizes measured in millimetres, ranging from zero point zero one to ten. The Y axis shows the percentage of passing particles, ranging from zero to one hundred percent. Three distinct lines are plotted, a solid black line for unwashed samples, a solid green line for washed samples, and dotted blue and red lines indicating upper and lower specification limits, respectively, cited from Vicroads, 2017 a. Data points for each line are represented by shapes, triangles for unwashed, squares for washed, and x marks for specification limits. The graph exhibits a consistent increase in percentage passing as the sieve size increases, with the unwashed samples consistently higher than the washed.Particle size distribution of unbound RCA and RG blend
Four FB-stabilised blends, utilising RTA as a secondary binder, were evaluated to assess their strength and stiffness for potential application in road construction. The results, presented in Table 3, were compared against a control blend in which 2% cement served as the secondary binder for FBS. As the RTA content increased, both the OMC and MDD decreased, as shown in Figure 8. The CBR values of the RCA + RG + 3% FB + 1% RTA and RCA + RG + 3% FB + 2% RTA blends were both 81%, which marginally met the LRA requirements for use in base and subbase applications. A previous investigation on comparable unbound RCA + RG mixes reported CBR values ranging from 116% to 147% (Maghool et al., 2021). The LRA’s Code of Practice specifies that recycled materials used in base or upper subbase layers must achieve a minimum CBR of 80%. In contrast, the Earthworks Specification allows values as low as 6% for materials used in capping, verges, structural fill, or select fill. Although blends containing more than 2% RTA did not meet the requirements for base or upper subbase layers, they demonstrated improved suitability for use in general fill applications (Vicroads, 2017a; Vicroads, 2015). However, unlike modulus, the CBR is an empirical value that does not directly correlate with any fundamental engineering property and is generally considered an indirect measure of shear strength. UCS tests were performed on FB-stabilised RCA and RG blends with varied RTA secondary binder contents, cured at temperatures of 20°C and 40°C for a period of 3 days, with the results, including those of the control blends, illustrated in Figure 9. Similar to the CBR results, UCS values decreased with increasing RTA content at both curing temperatures. In comparison to the control blend containing cement as the secondary binder, the blends incorporating RTA exhibited 90%–94% lower UCS values after 3 days of curing at 20°C, and 69%–77% lower UCS values after 3 days at 40°C. Meanwhile, the blends cured at 40°C exhibited a strength increase ranging from 13% to 24%. However, in pavement stabilisation, elevated UCS values result in increased stiffness, which can lead to issues with cracking.
OMC, MDD, CBR, UCS, and ITMr results of FB-stabilised blends with cement or RTA
| Blends | OMC: % | MDD: t/m2 | CBR: % | UCS 3-day 20°C: MPa | UCS 3-day 40°C: MPa | ITMr initial 3 h: MPa | ITMr 3-day (dried): MPa | ITMr 3-day (soaked): MPa | Retained resilient modulus |
|---|---|---|---|---|---|---|---|---|---|
| RCA + RG + 3% FB + 2% C | 9.20 | 2.081 | 430 | 1.510 | 2.063 | 1157 | 1514 | 797 | 0.53 |
| RCA + RG + 3% FB + 1% RTA | 9.20 | 2.081 | 81 | 0.156 | 0.484 | Failed | 1316 | 740 | 0.56 |
| RCA + RG + 3% FB + 2% RTA | 9.18 | 2.052 | 81 | 0.101 | 0.613 | Failed | 1210 | 955 | 0.79 |
| RCA + RG + 3% FB + 3% RTA | 9.15 | 2.047 | 72 | 0.107 | 0.641 | Failed | 1140 | 712 | 0.63 |
| RCA + RG + 3% FB + 4% RTA | 9.11 | 2.041 | 59 | 0.097 | 0.573 | Failed | 495 | 101 | 0.20 |
| Blends | OMC: % | MDD: t/m2 | CBR: % | ITMr initial 3 h: MPa | ITMr 3-day (dried): MPa | ITMr 3-day (soaked): MPa | Retained resilient modulus | ||
|---|---|---|---|---|---|---|---|---|---|
| 9.20 | 2.081 | 430 | 1.510 | 2.063 | 1157 | 1514 | 797 | 0.53 | |
| 9.20 | 2.081 | 81 | 0.156 | 0.484 | Failed | 1316 | 740 | 0.56 | |
| 9.18 | 2.052 | 81 | 0.101 | 0.613 | Failed | 1210 | 955 | 0.79 | |
| 9.15 | 2.047 | 72 | 0.107 | 0.641 | Failed | 1140 | 712 | 0.63 | |
| 9.11 | 2.041 | 59 | 0.097 | 0.573 | Failed | 495 | 101 | 0.20 |
The image contains two graphs titled O M C variation with R T A content and M D D variation with R T A content. The first graph, located at the top, presents O M C as a percentage on the vertical axis, ranging from nine point zero six to nine point two two, and displays data points for various blends labelled along the horizontal axis. The second graph, located below, shows M D D measured in square metres on the vertical axis, ranging from two point zero two to two point zero nine, against the same blend labels on the horizontal axis. Each graph features connected points that illustrate a trend for the data. The horizontal flow of the data indicates the changes in values across the specified blends.Variation of (a) OMC and (b) MDD with RTA content
The image contains two graphs titled O M C variation with R T A content and M D D variation with R T A content. The first graph, located at the top, presents O M C as a percentage on the vertical axis, ranging from nine point zero six to nine point two two, and displays data points for various blends labelled along the horizontal axis. The second graph, located below, shows M D D measured in square metres on the vertical axis, ranging from two point zero two to two point zero nine, against the same blend labels on the horizontal axis. Each graph features connected points that illustrate a trend for the data. The horizontal flow of the data indicates the changes in values across the specified blends.Variation of (a) OMC and (b) MDD with RTA content
The image presents a bar graph titled R C A plus R G plus F B plus R T A Stabilisation, illustrating the Unconfined Compressive Strength, U C S, measured in Megapascals, M P a. The vertical axis indicates the U C S values, ranging from zero to over two M P a, while the horizontal axis lists various mixtures, such as R C A plus R G plus 3 percent F B plus 2 percent C, and variations with different percentages of R T A. The graph distinguishes between two conditions, three days at twenty degrees Celsius and three days at forty degrees Celsius, with bars representing each condition. The bars in shades of grey represent the thirty degrees condition, while bars with a patterned fill represent the twenty degrees condition.UCS values of FB-stabilised blends with various RTA contents
The image presents a bar graph titled R C A plus R G plus F B plus R T A Stabilisation, illustrating the Unconfined Compressive Strength, U C S, measured in Megapascals, M P a. The vertical axis indicates the U C S values, ranging from zero to over two M P a, while the horizontal axis lists various mixtures, such as R C A plus R G plus 3 percent F B plus 2 percent C, and variations with different percentages of R T A. The graph distinguishes between two conditions, three days at twenty degrees Celsius and three days at forty degrees Celsius, with bars representing each condition. The bars in shades of grey represent the thirty degrees condition, while bars with a patterned fill represent the twenty degrees condition.UCS values of FB-stabilised blends with various RTA contents
ITMr tests were conducted on the control blend (RCA + RG + 3% FB + 2% C) after 3 h of drying at room temperature, 3 days of drying and curing at 40°C, and 3 days of drying and curing at 40°C followed soaking, as shown in Table 3. According to the LRA specifications, FB-stabilised materials should meet the following modulus requirements: an initial modulus greater than 700 MPa, a 3-day cured modulus between 2500 and 4000 MPa, and a soaked modulus between 1500 and 2000 MPa, and a retained modulus ratio greater than 0.5 (Vicroads, 2017b). The ITMr value for the FB-stabilised control blend satisfied the LRA’s requirement for the initial resilient modulus after 3 h. However, the control blend did not meet the required resilient modulus for both dried and soaked conditions after 3 days. All FB-stabilised blends containing RTA failed the ITMr tests after 3 h drying, and the results for all blends containing RTA for both dried and soaked conditions did not conform to the LRA's requirements. Insufficient adhesion and compatibility issues with FB can result in weak bonding, potentially lowering the material blends’ ITMr (Vicroads, 2016). The results are presented in Table 3 and Figure 10.
The image shows a bar chart titled R C A plus R G plus F B plus R T A Stabilisation that illustrates the Indirect Tensile Modulus, I T M t, values in Megapascals for different mixtures. The horizontal axis lists five mixtures involving Recycled Concrete Aggregate, R C A, Recycled Glass, R G, Foamed Bitumen, F B, and Reclaimed Asphalt, R T A, while the vertical axis represents modulus values ranging from zero to over two thousand five hundred Megapascals. Three sets of data are represented based on curing conditions, Initial 3 hours indicated by a blue striped pattern, 3 Days at 40 Degrees, Dried, shown in solid green, and 3 Days at 40 Degrees, Soaked, presented in solid yellow. The chart features three red dashed lines that mark significant modulus thresholds, 2,500 Megapascals for 3 Days Cured Modulus, 1,500 Megapascals for 3 Days Soaked Modulus, and 700 Megapascals for 3 Hours Initial Modulus. The data is arranged with bars corresponding to specific mixtures grouped together for comparison across different curing conditions.ITMr values of FB-stabilised blends with varying RTA contents after 3 h of drying, 3 days of drying, and 3 days of drying followed by soaking conditions
The image shows a bar chart titled R C A plus R G plus F B plus R T A Stabilisation that illustrates the Indirect Tensile Modulus, I T M t, values in Megapascals for different mixtures. The horizontal axis lists five mixtures involving Recycled Concrete Aggregate, R C A, Recycled Glass, R G, Foamed Bitumen, F B, and Reclaimed Asphalt, R T A, while the vertical axis represents modulus values ranging from zero to over two thousand five hundred Megapascals. Three sets of data are represented based on curing conditions, Initial 3 hours indicated by a blue striped pattern, 3 Days at 40 Degrees, Dried, shown in solid green, and 3 Days at 40 Degrees, Soaked, presented in solid yellow. The chart features three red dashed lines that mark significant modulus thresholds, 2,500 Megapascals for 3 Days Cured Modulus, 1,500 Megapascals for 3 Days Soaked Modulus, and 700 Megapascals for 3 Hours Initial Modulus. The data is arranged with bars corresponding to specific mixtures grouped together for comparison across different curing conditions.ITMr values of FB-stabilised blends with varying RTA contents after 3 h of drying, 3 days of drying, and 3 days of drying followed by soaking conditions
A series of laboratory tests was conducted to assess the strength and stiffness properties of FB-geopolymer-stabilised blends containing RCA and RG. These blends included 10%, 20%, and 30% of geopolymers made from FA, S, FA + S, used as secondary binders to enhance FBS. All test results are shown in Table 4. In all blends, increasing the proportion of each geopolymer secondary content led to a decrease in both OMC and MDD values, as anticipated and shown in Figure 11. FA, S geopolymers typically have lower specific gravities compared to RCA or RG. As greater amounts of these lighter materials are incorporated into the blend, the overall bulk density of the mixture decreases, leading to a lower MDD. Furthermore, the increased presence of fine geopolymer particles enhances particle packing by filling voids, which contributes to a reduced OMC (Lin et al., 2023). In many instances, stabilisation leads to a reduction in OMC compared to unbound material mixes (Lin et al., 2023). This reduction is commonly attributed to binder-induced changes, such as improved particle packing, which reduce the material's water absorption capacity. As OMC is influenced by various factors such binder composition, there is no standard OMC value for stabilised mixes. However, previous studies on similar unbound material blends have reported OMC values exceeding 10% (Maghool et al., 2021). In contrast, the stabilised mixes assessed in this study showed lower OMC values, ranging from 8.5% to 9.75%. With the exception of the S category, all geopolymer types demonstrated an increasing trend in CBR values as the proportion of the secondary binder increased, as illustrated in Figure 12. In contrast, increasing the S content from 20% to 30% negatively affected the workability of the mixture, likely due to the irregular shape of the S particles, which impeded uniform mixing and promoted agglomeration. Overall, all blends, except for RCA + RG + 3% FB + 10% FA, met the LRA's CBR requirement of 80%. Figure 13 illustrates the UCS test results for all blends containing geopolymers, as well as the control blend. In UCS tests, blends containing FA as a secondary binder demonstrated an increase in UCS values with higher FA content. The 3-day UCS values at 40°C were consistently higher than those at 20°C. Heating accelerates the pozzolanic reaction, enhancing cementation and increasing the strength of the stabilised material. The maximum UCS recorded was 2.713 MPa, achieved with the RCA + RG + 3% FB + 30% FA blend at 40°C. For blends using S as a secondary binder, UCS values decreased as the S content increased. Elevated temperatures did not enhance UCS for these blends; instead, UCS values decreased. Higher temperatures can speed up chemical reactions within the S, which might lead to a less stable interface with the bitumen and weaken the bonding strength. The maximum 3-day UCS recorded for S containing blends was 6.603 MPa, achieved with the RCA + RG + 3% FB + 10% S blend at 20°C. An increase in S and FA + S contents resulted in reduced workability, primarily due to the angular and irregular shape of the slag particles, which caused the material to agglomerate into a paste-like mass and hindered uniform mixing. Additionally, the rough surface texture of the slag particles diminished the effectiveness of FB coating, further compromising the integrity of the mix. These combined factors contributed to the observed reduction in UCS with increasing proportions of S and FA + S. In contrast, FA used alone, owing to its spherical particle morphology, facilitated more uniform mixing and improved coating efficiency, thereby enhancing the compressive strength of the stabilised material. The highest UCS value, 4.979 MPa, was obtained from the RCA + RG + 3% FB + 20%(FA + S) blend cured at 20°C. Blends incorporating 10% S, 20% S, 10% (FA + S), and 20% (FA + S) demonstrated significantly higher UCS values than the control blend at both 20°C and 40°C, where the control blend achieved 1.510 MPa and 2.063 MPa, respectively. Among the geopolymer types, S was the most effective secondary binder in enhancing the strength of the stabilised blends. FA is mainly composed of silica, alumina, and iron oxide, whereas S consisted predominantly of glassy phase materials along with crystalline calcite (Sun et al., 2024). The high calcium content in S increases its reactivity with moisture, leading to the formation of a stronger stabilised material.
OMC, MDD, CBR, UCS, and ITMr results of FB-stabilised blends with geopolymers
| Blends | OMC: % | MDD: t/m2 | CBR: % | UCS 3-day 20°C: MPa | UCS 3-day 40°C: MPa | ITMr initial 3-h: MPa | ITMr 3-day (dried): MPa | ITMr 3-day (soaked): MPa | Retained resilient modulus: % |
|---|---|---|---|---|---|---|---|---|---|
| RCA + RG + 3% FB + 10% FA | 8.98 | 2.079 | 36 | 0.272 | 0.879 | Failed | 2590 | 2525 | 0.97 |
| RCA + RG + 3% FB + 20% FA | 8.69 | 2.057 | 144 | 1.150 | 2.668 | 767 | 2797 | 1215 | 0.43 |
| RCA + RG + 3% FB + 30% FA | 8.56 | 2.005 | 291 | 2.022 | 2.713 | 1119 | 1920 | 688 | 0.39 |
| RCA + RG + 3% FB + 10% S | 9.72 | 2.124 | 686 | 6.603 | 5.420 | Failed | 2706 | 2106 | 0.78 |
| RCA + RG + 3% FB + 20% S | 9.36 | 2.098 | 739 | 6.174 | 4.081 | 1001 | 5232 | 1529 | 0.29 |
| RCA + RG + 3% FB + 30% S | 9.17 | 2.093 | 595 | 1.098 | 1.418 | 548 | 1880 | 915 | 0.49 |
| RCA + RG + 3% FB + 10%(FA + S) | 9.13 | 2.116 | 364 | 4.782 | 4.185 | Failed | 5672 | 4390 | 0.77 |
| RCA + RG + 3% FB + 20%(FA + S) | 8.79 | 2.091 | 534 | 4.979 | 3.059 | 1000 | 3521 | 2601 | 0.74 |
| RCA + RG + 3% FB + 30%(FA + S) | 8.67 | 2.057 | 864 | 0.476 | 0.720 | 759 | 1988 | 929 | 0.47 |
| Blends | OMC: % | MDD: t/m2 | CBR: % | ITMr initial 3-h: MPa | ITMr 3-day (dried): MPa | ITMr 3-day (soaked): MPa | Retained resilient modulus: % | ||
|---|---|---|---|---|---|---|---|---|---|
| 8.98 | 2.079 | 36 | 0.272 | 0.879 | Failed | 2590 | 2525 | 0.97 | |
| 8.69 | 2.057 | 144 | 1.150 | 2.668 | 767 | 2797 | 1215 | 0.43 | |
| 8.56 | 2.005 | 291 | 2.022 | 2.713 | 1119 | 1920 | 688 | 0.39 | |
| 9.72 | 2.124 | 686 | 6.603 | 5.420 | Failed | 2706 | 2106 | 0.78 | |
| 9.36 | 2.098 | 739 | 6.174 | 4.081 | 1001 | 5232 | 1529 | 0.29 | |
| 9.17 | 2.093 | 595 | 1.098 | 1.418 | 548 | 1880 | 915 | 0.49 | |
| 9.13 | 2.116 | 364 | 4.782 | 4.185 | Failed | 5672 | 4390 | 0.77 | |
| 8.79 | 2.091 | 534 | 4.979 | 3.059 | 1000 | 3521 | 2601 | 0.74 | |
| 8.67 | 2.057 | 864 | 0.476 | 0.720 | 759 | 1988 | 929 | 0.47 |
The image features two line graphs, one titled O M C variation with Geopolymer content and the other titled M D D variation with Geopolymer content. The upper graph indicates the O M C percentage on the vertical axis ranging from seven point eighty to ten and shows percentages of geopolymer on the horizontal axis at intervals of ten, twenty, and thirty. It illustrates four lines representing different compositions with distinct colour coding, orange for R C A plus R G plus three percent F B plus F A, green for R C A plus R G plus three percent F B plus S, purple for R C A plus R G plus three percent F B plus F A plus S, and a fourth composition indicated by a different colour. The lower graph represents the M D D in terms of tons per square metre, with values ranging from one point ninety four to two point fourteen, using the same percentage distribution along the horizontal axis. Both graphs feature markers on the lines, allowing for precise value identification, and the lines consistently trend downwards as the geopolymer percentage increases.Variation of (a) OMC and (b) MDD with geopolymer content
The image features two line graphs, one titled O M C variation with Geopolymer content and the other titled M D D variation with Geopolymer content. The upper graph indicates the O M C percentage on the vertical axis ranging from seven point eighty to ten and shows percentages of geopolymer on the horizontal axis at intervals of ten, twenty, and thirty. It illustrates four lines representing different compositions with distinct colour coding, orange for R C A plus R G plus three percent F B plus F A, green for R C A plus R G plus three percent F B plus S, purple for R C A plus R G plus three percent F B plus F A plus S, and a fourth composition indicated by a different colour. The lower graph represents the M D D in terms of tons per square metre, with values ranging from one point ninety four to two point fourteen, using the same percentage distribution along the horizontal axis. Both graphs feature markers on the lines, allowing for precise value identification, and the lines consistently trend downwards as the geopolymer percentage increases.Variation of (a) OMC and (b) MDD with geopolymer content
The line graph displays the variation of California Bearing Ratio percentage labelled as C B R against Geopolymer percentages of ten percent, twenty percent, and thirty percent on the horizontal axis, with values ranging from zero percent to one thousand percent on the vertical axis. Four lines represent distinct combinations of materials, R C A plus R G plus three percent F B plus F A, depicted in orange, R C A plus R G plus three percent F B plus S, shown in green, R C A plus R G plus three percent F B plus an additional F A and S, represented by a purple line, and the combination of R C A plus R G plus three percent F B plus F A and S is illustrated with a green line. The data flows along the horizontal axis from left to right, while the vertical axis displays data from bottom to top.CBR variation with geopolymer content
The line graph displays the variation of California Bearing Ratio percentage labelled as C B R against Geopolymer percentages of ten percent, twenty percent, and thirty percent on the horizontal axis, with values ranging from zero percent to one thousand percent on the vertical axis. Four lines represent distinct combinations of materials, R C A plus R G plus three percent F B plus F A, depicted in orange, R C A plus R G plus three percent F B plus S, shown in green, R C A plus R G plus three percent F B plus an additional F A and S, represented by a purple line, and the combination of R C A plus R G plus three percent F B plus F A and S is illustrated with a green line. The data flows along the horizontal axis from left to right, while the vertical axis displays data from bottom to top.CBR variation with geopolymer content
The image features three bar graphs presented vertically, labelled a, b, and c. Each graph compares unconfined compressive strength, measured in megapascals, of various mixtures containing recycled concrete aggregates, R C A, rubber granules, R G, fibrous materials, F B, and additional materials like fly ash, F A, or silica, S. The X axis lists the mixture compositions, while the Y axis shows compressive strength values ranging from zero to a maximum value indicated by the tallest bar. Each mixture shows two bars, one representing measurements taken at twenty degrees Celsius and another at forty degrees Celsius, differentiated by solid and hatched patterns. Data is organised from left to right, with varying compositions affecting the height of the bars visibly.UCS values for the control blend and FB-stabilised blends with secondary binders: (a) FA, (b) S, (c) FA + S
The image features three bar graphs presented vertically, labelled a, b, and c. Each graph compares unconfined compressive strength, measured in megapascals, of various mixtures containing recycled concrete aggregates, R C A, rubber granules, R G, fibrous materials, F B, and additional materials like fly ash, F A, or silica, S. The X axis lists the mixture compositions, while the Y axis shows compressive strength values ranging from zero to a maximum value indicated by the tallest bar. Each mixture shows two bars, one representing measurements taken at twenty degrees Celsius and another at forty degrees Celsius, differentiated by solid and hatched patterns. Data is organised from left to right, with varying compositions affecting the height of the bars visibly.UCS values for the control blend and FB-stabilised blends with secondary binders: (a) FA, (b) S, (c) FA + S
ITMr tests were performed on the FB-stabilised blends incorporated with FA, S, and FA + S, and the test results are presented in Figure 14. The 3-day dried samples exhibited the highest ITMr values compared to those dried for 3 h or dried for 3 days followed by soaking, regardless of their composition. FB-stabilised blends containing FA (10%, 20%, and 30%) did not conform with LRA specifications. The blend of RCA + RG + 3% FB + 20% S achieved resilient modulus values of 1,001 MPa after 3 h of drying, 5,232 MPa after 3 days of drying, and 1,529 MPa after 3 days of drying followed by soaking. These values met the LRA requirements but did not satisfy the retained resilient modulus criteria. The blend of RCA + RG + 3% FB + 20%(FA + S) achieved resilient modulus values of 1,000 MPa, 3,521 MPa, and 2,601 MPa under 3-hour drying, 3-day drying, and 3-day drying followed by soaking, respectively. The blend exhibited a retained resilient modulus of 0.74, and therefore, it satisfies all the requirements set forth by the LRA specifications. Compared to dried samples, wet conditioning can cause water ingress into the partially formed binder matrix, weakening interparticle bonds. This leads to reduced cohesion and elasticity of the blend, thereby directly decreasing the tensile modulus. FB forms a stabilising film around the aggregates; however, in the presence of excess moisture, adhesion between the bitumen and aggregates deteriorates, resulting in a loss of stiffness and resilient modulus (Vinet-Cantot et al., 2019). FBS involves reducing stiffness and enhancing the flexibility of the bound layer, which improves its fatigue resistance (Ramanujam and Jones, 2007). The ITMr offers an indirect measure of fatigue resistance by assessing stiffness under tensile stress. Therefore, 20%(FA + S) is recommended as secondary binders for FBS in pavement applications.
This image displays three bar graphs labelled a, b, and c, each titled R C A plus R G plus F B plus F A Stabilisation or similar variations. The Y axis represents the strength measured in mega pascals, M P a, and horizontal reference lines indicate performance thresholds for 3 Days Cured, 3 Days Soaked, and 3 Hours Initial. Each graph presents different mixtures and their measured strengths, specifically contrasting the strength at three durations, Initial 3 hours, 3 Days at 40 Degrees, Dried, and 3 Days at 40 Degrees, Soaked. The bars vary in height, indicating distinct results based on composition, which includes parameters such as percentages of F B and F A. Each bar is colour coded, with a legend indicating the meaning of the colours, and red dashed lines help highlight the set benchmarks referenced from sources.ITMr values of FB-stabilised blends with varying contents of (a) FA, (b) S, and (c) FA + S, measured after 3 h of drying, 3 days of drying, and 3 days of drying followed by soaking conditions
This image displays three bar graphs labelled a, b, and c, each titled R C A plus R G plus F B plus F A Stabilisation or similar variations. The Y axis represents the strength measured in mega pascals, M P a, and horizontal reference lines indicate performance thresholds for 3 Days Cured, 3 Days Soaked, and 3 Hours Initial. Each graph presents different mixtures and their measured strengths, specifically contrasting the strength at three durations, Initial 3 hours, 3 Days at 40 Degrees, Dried, and 3 Days at 40 Degrees, Soaked. The bars vary in height, indicating distinct results based on composition, which includes parameters such as percentages of F B and F A. Each bar is colour coded, with a legend indicating the meaning of the colours, and red dashed lines help highlight the set benchmarks referenced from sources.ITMr values of FB-stabilised blends with varying contents of (a) FA, (b) S, and (c) FA + S, measured after 3 h of drying, 3 days of drying, and 3 days of drying followed by soaking conditions
Conclusions
This laboratory-based experimental study was conducted to investigate the strength and stiffness properties of FB-stabilised blends containing 50% RCA and 50% RG, supplemented individually with various secondary binders, including RTA and the geopolymers FA, S, and FA + S.
CBR testing showed that the blends only marginally meet the LRA specification requirements, even when 1%–2% RTA is used as a secondary binder. UCS values are significantly lower compared to the control blend, even at increased 40°C temperature curing. The results for all blends containing RTA, under both dried and soaked conditions, failed to meet the LRA’s requirements. RTA, which is typically composed of carbon and soft plastic, does not provide the same bonding properties as traditional binders like cement or hydrated lime. This weaker bonding reduces the overall strength of the stabilised material, leading to lower CBR and UCS values. The components in RTA contribute to reduced elasticity, lowering stiffness and, consequently, the ITMr values. The chemical composition of RTA can also vary significantly between different brands and types, making it difficult to ensure consistent quality. While the FB-stabilised RCA and RG blends with RTA do not fully meet the base LRA specifications for even roads with Equivalent Standard Axles less than 100, these blends are still overqualified for use in applications such as fills.
When performing FBS with FA, S, and FA + S as secondary binder geopolymers, each material behaves differently. With FA, increasing its content generally enhances both the CBR and UCS due to FA’s pozzolanic characteristics, and UCS values improve with higher temperatures. In contrast, increasing the S content tends to reduce both CBR and UCS, as S forms coarser crystalline structures that do not integrate as effectively with FB. Higher S levels can result in a more brittle, less flexible pavement structure, and unlike FA, UCS values with S do not improve at higher temperatures. In ITMr tests, the blend RCA + RG + 3% FB + 20%(FA + S) met LRA specification requirements, demonstrating suitability for pavement stabilisation as an alternative to conventional high carbon-emitting methods.
Field trials may verify the effectiveness of the secondary binders mentioned above. However, several past laboratory and field comparisons of FBS have indicated that the field resilient modulus closely matches the soaked resilient modulus observed in the laboratory (Ramanujam and Jones, 2007). Based on the findings, it is recommended to use 20%(FA + S) as a secondary binder for the FBS of pavements containing RCA and RG.
CRediT authorship contribution statement
Muditha Senanayake: conceptualisation, investigation, methodology, software, writing – original draft. Youli Lin: conceptualisation, investigation, writing – review and editing. Arul Arulrajah: conceptualisation, resources, supervision, funding acquisition, writing – review and editing. Farshid Maghool: conceptualisation, resources, supervision, funding acquisition, writing – review and editing. Suksun Horpibulsuk: conceptualisation, writing – review and editing.

